Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 3,7-Dichloroquinolin-8-carbonyl Chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | Quinclorac | HCID 91739 | — |
| 생성물 | 3,7-Dichloroquinolin-8-carbonyl Chloride | HCID 13090840 | 95.7% |
반응 단계
3,7-Dichloro-8-quinolinecarboxylic acid(20 g, 82 mmol) was added to thionyl chloride(80 ml), and the mixture refluxed for 3 hours and concentrated under reduced pressure to afford the desired product(20.6 g, yield=95.7%) as a light brown solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05489687 |
| 출처 데이터셋 | uspto-grants-1996_02 |
| ORD ID | ord-a3d5fd81fa9442d3a1d98dde0c6573c8 |
| 출처 메모 | uspto-grants-1996_02 |