Trifluoroacetic acid → HCID 19974025, 화합물
반응식
C(OC([NH:8][CH2:9][CH2:10][N:11]([C:15](=[O:20])[C:16]([F:19])([F:18])[F:17])[CH2:12][CH:13]=[CH2:14])=O)(C)(C)C.[F:21][C:22]([F:27])([F:26])[C:23]([OH:25])=[O:24]>C(Cl)Cl>[F:21][C:22]([F:27])([F:26])[C:23]([OH:25])=[O:24].[F:17][C:16]([F:18])([F:19])[C:15]([N:11]([CH2:12][CH:13]=[CH2:14])[CH2:10][CH2:9][NH2:8])=[O:20]참가 물질
4
실험 절차
Dissolve N-(t-butyloxycarbonyl)-N'-(trifluoroacetyl)-N'-(allyl)-ethylenediamine (1.95 mmol) in methylene chloride (7 mL) and add trifluoroacetic acid (2.6mL). Stir at room temperature for 1 hour then evaporate the solvent in vacuo to give N'-(trifluoroacetyl)-N'-(allyl)-ethylenediamine trifluoroacetate.
후처리
- customthen evaporate the solvent in vacuo
출처 및 근거
- ORD 기록
- ord-e1c8eded093d49f099010282bc3277f5
- 출처 데이터셋
- uspto-grants-1996_02
- 특허 번호
- US05491141
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