Ethanol → Ethyl sulfoacetate

HRID 2396092노트

반응식

HRID 2396092 반응식
[S:1]([CH2:5][C:6]([OH:8])=[O:7])([OH:4])(=[O:3])=[O:2].[CH3:9][CH2:10]O>>[S:1]([CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7])([OH:4])(=[O:3])=[O:2]

참가 물질

3

반응물 2

HCID 702EthanolHCID 31257Sulfoacetic acid

생성물 1

HCID 12216623Ethyl sulfoacetate

실험 절차

Sulfoacetic acid (52 g, 371 mM) and EtOH (500 mL) were heated under reflux for 20 hours. The reaction mixture was cooled, and the excess ethanol was removed under vacuum to give ethyl sulfoacetate.

후처리

  1. temperatureunder reflux for 20 hours
  2. temperatureThe reaction mixture was cooled
  3. customthe excess ethanol was removed under vacuum

출처 및 근거

ORD 기록
ord-292b72945d0e454c82fdb19175274c63
출처 데이터셋
uspto-grants-1996_02
특허 번호
US05491170

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