Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 4,4,6-Trimethyl-1,3,2-dioxaborinan-2-OL
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Boric Acid | HCID 7628 | — |
| 반응물 | Hexylene Glycol | HCID 7870 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 4,4,6-Trimethyl-1,3,2-dioxaborinan-2-OL | HCID 352515 | — |
반응 단계
Boric acid (1mole) and 2methyl-2,4-pentanediol (1mole) were placed in a reaction vessel with 1,000 ml of benzene and the mixture refluxed until 2 moles of water were removed. Evaporation of the benzene at reduced pressure gave a liquid which slowly crystallized to give a white solid mp 73-75° C. [literature mp 69°-70° C. C. H. Steinberg and D. L. Hunter, Ind. & Eng. Chem. 49, 174-181 (1957)].
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04021407 |
| 출처 데이터셋 | uspto-grants-1977_05 |
| ORD ID | ord-38930afadfe04d7f8316dd46cb3261ca |
| 출처 메모 | uspto-grants-1977_05 |