Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzoic Acid → 3,7-Dimethylocta-2,6-Dienal
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzoic Acid | HCID 243 | — |
| 반응물 | Prenyl acetate | HCID 14489 | — |
| 반응물 | 3-Methyl-2-butenal | HCID 61020 | — |
| 생성물 | 3,7-Dimethylocta-2,6-Dienal | HCID 8843 | 48% |
반응 단계
60 parts of prenyl acetate, 40 parts of 3,3-dimethylacrolein and 2 parts of benzoic acid are heated together for five hours 30 minutes at 140° C and the product is worked up. 11.1 parts of citral is obtained having a boiling point of 104° C. at 12 mm in a yield of 48% at a conversion of 32% (based on 3,3-dimethylacrolein).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04021411 |
| 출처 데이터셋 | uspto-grants-1977_05 |
| ORD ID | ord-e57109bcc24a4a4c974ad32242a7c820 |
| 출처 메모 | uspto-grants-1977_05 |