Tetralin → 1-Amino-8-chloroanthraquinone

HRID 2397262

반응식

HRID 2397262 반응식
[N+:1]([C:4]1[C:17]2[C:16](=[O:18])[C:15]3[C:10](=[CH:11][CH:12]=[CH:13][C:14]=3[Cl:19])[C:9](=[O:20])[C:8]=2[CH:7]=[CH:6][CH:5]=1)([O-])=O.C1C2C(=CC=CC=2)CCC1>>[NH2:1][C:4]1[C:17]2[C:16](=[O:18])[C:15]3[C:10](=[CH:11][CH:12]=[CH:13][C:14]=3[Cl:19])[C:9](=[O:20])[C:8]=2[CH:7]=[CH:6][CH:5]=1

참가 물질

3

반응물 2

HCID 8404TetralinHCID 2257041-Nitro-8-chloroanthraquinone

생성물 1

HCID 2236691-Amino-8-chloroanthraquinone

실험 절차

28.8 parts of 1-nitro-8-chloroanthraquinone are heated for 5 hours at boiling temperature in 160 parts of tetrahydronaphthalene. The remainder of the process is carried out as described in Example 4 to yield 20.2 parts of 1-amino-8-chloroanthraquinone.

출처 및 근거

ORD 기록
ord-332e0fcc3fb24c079510518166b150e8
출처 데이터셋
uspto-grants-1977_05
특허 번호
US04021456

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