Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Propane sultone → Agn-PC-006bky
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Propane sultone | HCID 14264 | — |
| 반응물 | (3,5-Dimethoxyphenyl)methanamine | HCID 420973 | — |
| 용매 | Methyl Ethyl Ketone | HCID 6569 | — |
| 생성물 | Agn-PC-006bky | HCID 11300729 | — |
반응 단계
To a solution of 3,5-dimethoxybenzylamine (2.5 g, 15.0 mmol) in 2-butanone (22 mL) was added 1,3-propane sultone (1.95 g, 15.8 mmol). The mixture was stirred at reflux for 2 hours. The reaction mixture was cooled to room temperature. The solid was collected by filtration, washed with acetone (2×25 mL), and dried in vacuo. This allowed the isolation of compound BA, 2.89 g (67%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08642801B2 |
| 출처 데이터셋 | uspto-grants-2014_02 |
| ORD ID | ord-7dd78b3b7325462089c01f762ca08271 |
| 출처 메모 | uspto-grants-2014_02 |