Propane sultone → 3-((1-Methylcyclopentyl)amino)propane-1-sulfonic acid

HRID 239783노트

반응식

HRID 239783 반응식
[CH2:1]1[CH2:7][S:4](=[O:6])(=[O:5])[O:3][CH2:2]1.[CH3:8][C:9]1([NH2:14])[CH2:13][CH2:12][CH2:11][CH2:10]1>CC(=O)CC>[CH3:8][C:9]1([NH:14][CH2:2][CH2:1][CH2:7][S:4]([OH:3])(=[O:6])=[O:5])[CH2:13][CH2:12][CH2:11][CH2:10]1

참가 물질

4

반응물 2

HCID 14264Propane sultoneHCID 520998Cyclopentanamine, 1-methyl-

생성물 1

HCID 160358473-((1-Methylcyclopentyl)amino)propane-1-sulfonic acid

시약·촉매·용매 1

HCID 6569Methyl Ethyl Ketone용매

실험 절차

A solution of 1,3-propanesultone (9.4 g, 75 mmol) in 2-butanone (35 mL) was added dropwise to a the crude solution of 1-methyl-1-cyclopentylamine (mixture of solvent from previous step).

출처 및 근거

ORD 기록
ord-66bb6a4238b34d41bba2199ffc7e2a15
출처 데이터셋
uspto-grants-2014_02
특허 번호
US08642801B2

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