Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzoyl chloride, 3,4,5-trimethoxy- → 6-(3,4,5-Trimethoxybenzamido)-2-methyl-1,2,3,4-tetrahydroisoquinoline
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzoyl chloride, 3,4,5-trimethoxy- | HCID 78282 | — |
| 반응물 | 2-Methyl-1,2,3,4-tetrahydroisoquinolin-6-amine | HCID 21436741 | — |
| 생성물 | 6-(3,4,5-Trimethoxybenzamido)-2-methyl-1,2,3,4-tetrahydroisoquinoline | HCID 216593 | — |
반응 단계
6-Amino-2-methyl-1,2,3,4-tetrahydroisoquinoline was reacted with 3,4,5-trimethoxybenzoyl chloride as in Example 16 to yield 6-(3,4,5-trimethoxybenzamido)-2-methyl-1,2,3,4-tetrahydroisoquinoline. It was recovered as the HCl salt; m.p. 233.5°-235° C. after purification in methanol.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04022900 |
| 출처 데이터셋 | uspto-grants-1977_05 |
| ORD ID | ord-bec9069431bb45fc91c40e6826400640 |
| 출처 메모 | uspto-grants-1977_05 |