Butyl isocyanate → 2-Acryloyloxyethyl butylcarbamate

반응식

[CH2:1]([N:5]=[C:6]=[O:7])[CH2:2][CH2:3][CH3:4].[C:8]([O:12][CH2:13][CH2:14][OH:15])(=[O:11])[CH:9]=[CH2:10].COC1C=CC(O)=CC=1>>[C:8]([O:12][CH2:13][CH2:14][O:15][C:6](=[O:7])[NH:5][CH2:1][CH2:2][CH2:3][CH3:4])(=[O:11])[CH:9]=[CH2:10]

참가 물질

반응물 3

HCID 8110Butyl isocyanate

HCID 90154-Methoxyphenol

HCID 131652-Hydroxyethyl acrylate

생성물 1

HCID 1131592-Acryloyloxyethyl butylcarbamate

실험 절차

145.3 grams of butyl isocyanate and 180.7 grams of 2-hydroxyethyl acrylate, stabilized with 400 ppm of hydroquinone monomethyl ether, were reacted together for 6 hours at 75° C. to give 1-butane carbamic acid 2-acryloyloxyethyl ester.

후처리

customwere reacted together for 6 hours at 75° C.

출처 및 근거

ORD 기록: ord-246445da7f0242cd95eb8ddd65e90a62
출처 데이터셋: uspto-grants-1977_05
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04023208

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