4,5-Dichloro-2-nitroaniline → 11,12-Dichlorodibenzo(a,c)phenazine
반응식
[Cl:1][C:2]1[CH:3]=[C:4]([C:6]([N+:10]([O-])=O)=[CH:7][C:8]=1[Cl:9])[NH2:5].[C:13]1(=O)[C:26]2[CH:25]=[CH:24][C:23]3[C:18](=[CH:19][CH:20]=[CH:21][CH:22]=3)[C:17]=2[CH:16]=[CH:15][C:14]1=O>CN(C=O)C>[Cl:1][C:2]1[CH:3]=[C:4]2[C:6](=[CH:7][C:8]=1[Cl:9])[N:10]=[C:25]1[C:24]([C:23]3[CH:22]=[CH:21][CH:20]=[CH:19][C:18]=3[C:17]3[CH:16]=[CH:15][CH:14]=[CH:13][C:26]=31)=[N:5]2참가 물질
4
실험 절차
When 0.14 mole each of 3,4-dichloro-6-nitroaniline and phenanthrenequinone were reacted by the method of Example 1, 48.8 g. (99.9 percent yield) of 11,12-dichlorodibenzo[a,c]phenazine, mp = 263°-264° C. (DMF), were obtained.
출처 및 근거
- ORD 기록
- ord-62b8c8a835d541b7b4d1a587c295f832
- 출처 데이터셋
- uspto-grants-1977_05
- 특허 번호
- US04024142
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