Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Methoxybenzenesulfonyl chloride → N-(2-benzoyl-4-bromo-phenyl)-4-methoxy-benzenesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Methoxybenzenesulfonyl chloride | HCID 7401 | — |
| 반응물 | 2-Amino-5-bromobenzophenone | HCID 99677 | — |
| 생성물 | N-(2-benzoyl-4-bromo-phenyl)-4-methoxy-benzenesulfonamide | HCID 9955192 | — |
반응 단계
The title compound was prepared according to the general procedure for the synthesis of N-Aryl-benzenesulfonamides previously described using 138 mg of (2-Amino-5-bromo-phenyl)-phenyl-methanone and 103 mg of 4-Methoxy-benzenesulfonyl chloride. 1H-NMR (400 MHz, CDCl3): δ 3.78 (s, 3H), 6.83 (d, 2H, J=9.2 Hz), 7.39 (b, 1H), 7.49 (d, 2H, J=6.4 Hz), 7.68 (m, 4H), 8.85 (d, 2H, J=6.0 Hz), 9.96 (b, 1H). MS: m/z 447.0 (M++1).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08642808B2 |
| 출처 데이터셋 | uspto-grants-2014_02 |
| ORD ID | ord-39a15ca559334bffbb7439747cde7be0 |
| 출처 메모 | uspto-grants-2014_02 |