Ammonium Hydroxide → alpha-Amino-9H-xanthene-9-acetic acid

HRID 2399624노트

반응식

HRID 2399624 반응식
Cl.[NH2:2][CH:3]([CH:7]1[C:20]2[CH:19]=[CH:18][CH:17]=[CH:16][C:15]=2[O:14][C:13]2[C:8]1=[CH:9][CH:10]=[CH:11][CH:12]=2)[C:4]([OH:6])=[O:5].[OH-].[NH4+]>O>[NH2:2][CH:3]([CH:7]1[C:8]2[CH:9]=[CH:10][CH:11]=[CH:12][C:13]=2[O:14][C:15]2[C:20]1=[CH:19][CH:18]=[CH:17][CH:16]=2)[C:4]([OH:6])=[O:5]

참가 물질

4

반응물 2

HCID 14923Ammonium HydroxideHCID 67805111alpha-Amino-9H-xanthene-9-acetic acid hydrochloride

생성물 1

HCID 9816503alpha-Amino-9H-xanthene-9-acetic acid

시약·촉매·용매 1

HCID 962Water용매

실험 절차

α-Amino-9H-xanthene-9-acetic acid hydrochloride is dissolved in water and the pH of the solution is adjusted with dilute ammonium hydroxide solution to pH 7. The precipitate is collected by filtration, washed with water, boiled with water for a short time, cooled to room temperature, and collected to afford the title compound.

후처리

  1. filtrationThe precipitate is collected by filtration
  2. washwashed with water
  3. customcollected

출처 및 근거

ORD 기록
ord-c1b034a176ed4240bfc389bf4660c25b
출처 데이터셋
uspto-grants-1995_09
특허 번호
US05449778

반응 노트

불러오는 중…