Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Myristyl chloride → Tetradecyl-[3-(p-Dimethylaminobenzamido)propyl]-Dimethylammonium Chloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Myristyl chloride | HCID 17043 | — |
| 반응물 | 4-(dimethylamino)-N-[3-(dimethylamino)propyl]benzamide | HCID 3978888 | — |
| 생성물 | Tetradecyl-[3-(p-Dimethylaminobenzamido)propyl]-Dimethylammonium Chloride | HCID 15825621 | — |
반응 단계
50 g of N-(3-dimethylaminopropyl)-p-dimethylaminobenzamide (0.201 mole) from Example 1 and 47 g of tetradecylchloride (0.195 mole) were melted together and kept at 130° C. for 4 hours. Product was crystallized from 250 ml of ethylacetate; the crystals were washed with another 150 ml of ethylacetate. Yield was 71 g (74% of theoretical yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05451394 |
| 출처 데이터셋 | uspto-grants-1995_09 |
| ORD ID | ord-caf60ebe87a6448e9d4e4e1649dbf069 |
| 출처 메모 | uspto-grants-1995_09 |