Ethylamine → HCID 19382186, 화합물

HRID 2400076노트

반응식

HRID 2400076 반응식
[O:1]1[C:3]2([CH2:8][CH2:7][N:6]([C:9]([O:11][CH2:12][CH3:13])=[O:10])[CH2:5][CH2:4]2)[CH2:2]1.[CH2:14]([NH2:16])[CH3:15]>>[CH2:14]([NH:16][CH2:2][C:3]1([OH:1])[CH2:8][CH2:7][N:6]([C:9]([O:11][CH2:12][CH3:13])=[O:10])[CH2:5][CH2:4]1)[CH3:15]

참가 물질

3

반응물 2

HCID 6341EthylamineHCID 13672926Ethyl 1-oxa-6-azaspiro[2,5]octane-6-carboxylate

생성물 1

HCID 19382186HCID 19382186, 화합물

실험 절차

5.7 g (30.8 mmol) of ethyl 6-aza-1-oxaspiro[2,5]octane-6-carboxylate are added dropwise to 30 ml of ethylamine solution (50% in water) and the mixture is stirred overnight at room temperature. It is then concentrated and distilled.

후처리

  1. concentrationIt is then concentrated
  2. distillationdistilled

출처 및 근거

ORD 기록
ord-316e70911c3348dbab823113457d1988
출처 데이터셋
uspto-grants-1995_09
특허 번호
US05453422

반응 노트

불러오는 중…