Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(Benzylamino)pyridine → N-(3-{4-[(Benzyl-pyridin-2-yl-amino)-methyl]-phenyl}-pyrazin-2-yl)-2-chloro-benzenesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(Benzylamino)pyridine | HCID 23362 | — |
| 반응물 | HCID 57444254 | HCID 57444254 | — |
| 생성물 | N-(3-{4-[(Benzyl-pyridin-2-yl-amino)-methyl]-phenyl}-pyrazin-2-yl)-2-chloro-benzenesulfonamide | HCID 11960665 | 35% |
반응 단계
Following the general method as outlined in Example 1 (Method B), starting from N-{3-[4-(chloromethyl)phenyl]pyrazin-2-yl}-2-(chloro) benzenesulfonamide (Intermediate 8), and 2-benzylaminopyridine, the title compound was isolated as a yellow solid in 35% yield (94% purity by HPLC).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08796280B2 |
| 출처 데이터셋 | uspto-grants-2014_08 |
| ORD ID | ord-6cf549fa2c954c6c921392dc272dfe8c |
| 출처 메모 | uspto-grants-2014_08 |