Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → 3-methoxy-9-oxo-9H-indeno[1,2-b]pyrazine-2-carbonitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | 9-oxo-9H-indeno(1,2-b)pyrazine-2,3-dicarbonitrile | HCID 292929 | — |
| 생성물 | 3-methoxy-9-oxo-9H-indeno[1,2-b]pyrazine-2-carbonitrile | HCID 16065353 | 126.5% |
반응 단계
To a suspension of 1 (1.10 g, 4.7 mmol) in MeOH (47 ml) sodium (110 mg) was added and the mixture was stirred at room temperature for 16 hours. The precipitate was filtered, washed with EtOH and dried under vacuum, yielding 3 (1.03 g, 93%) as yellow-green solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08648076B2 |
| 출처 데이터셋 | uspto-grants-2014_02 |
| ORD ID | ord-b40012b19977406f87d5a10b4b6e4989 |
| 출처 메모 | uspto-grants-2014_02 |