Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → 2-Methylindan-2-yl methacrylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | Methacryloyl chloride | HCID 13528 | — |
| 반응물 | 2-Methyl-2-indanol | HCID 569220 | — |
| 용매 | Toluene | HCID 1140 | — |
| 생성물 | 2-Methylindan-2-yl methacrylate | HCID 86676054 | — |
반응 단계
With stirring and ice cooling, 111 g of triethylamine was added to a mixture of 120 g of methacrylic acid chloride, 200 g of 2-methyl-2-hydroxyindane, and 1500 g of toluene. The mixture was stirred at room temperature for 16 hours. By standard aqueous work-up and solvent distillation, a crude product was obtained. It was purified by column chromatography, yielding the target compound, 2-methylindan-2-yl methacrylate, designated Monomer 1.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08808966B2 |
| 출처 데이터셋 | uspto-grants-2014_08 |
| ORD ID | ord-fc74241a160b4f8fb760d6aa0848426a |
| 출처 메모 | uspto-grants-2014_08 |