참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-Amino-5-nitrobenzoic acid | HCID 12032 | — |
| 반응물 | Formamidine acetate | HCID 160693 | — |
| 용매 | 1-Methoxyethanol | HCID 3015637 | — |
| 생성물 | HCID 178526470 | HCID 178526470 | — |
반응 단계
A mixture of 2-amino-5-nitrobenzoic acid (1000 g, 5 mol) and formamidine acetate (1000 g, 10 mol) were dissolved in methoxyethanol (4 L) and heated to 115° C. for 16 hours. After cooling the mixture to room temperature, ice water (5 L) was added and the mixture was stirred for 30 minutes before collecting the product (125 g, 14%) by filtration.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08648087B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_02 |
|---|
| ORD ID | ord-c6eaa425e0df4e24ab878d970d8aa4c3 |
|---|
| 출처 메모 | uspto-grants-2014_02 |
|---|
