HCID 23146084, 화합물 → 1-(4-(2-(Dimethylamino)ethoxy)phenyl)butan-1-amine

HRID 2406577노트

반응식

HRID 2406577 반응식
[CH2:1]([N:3]([CH2:18]C)[CH2:4][CH2:5][O:6][C:7]1[CH:12]=[CH:11][C:10]([CH:13]([NH2:17])[CH2:14][CH2:15][CH3:16])=[CH:9][CH:8]=1)C.CN(C)CCOC1C=CC(C(=O)CCC)=CC=1>>[CH3:18][N:3]([CH3:1])[CH2:4][CH2:5][O:6][C:7]1[CH:8]=[CH:9][C:10]([CH:13]([NH2:17])[CH2:14][CH2:15][CH3:16])=[CH:11][CH:12]=1

참가 물질

3

반응물 2

HCID 23146084HCID 23146084, 화합물HCID 66822143HCID 66822143, 화합물

생성물 1

HCID 668222551-(4-(2-(Dimethylamino)ethoxy)phenyl)butan-1-amine수율 73%

실험 절차

The title compound was prepared by using a similar procedure as described for the preparation of 25 except that 1-(4-(2-(dimethylamino)ethoxy)phenyl)butan-1-one (22) was used instead of 1-(4-(2-(diethylamino)ethoxy)phenyl)butan-1-one (21). This produced crude 26 (410 mg, 73%) as a yellow oil: MS (ES+) m/z 237.1 (M+H)+.

후처리

  1. customThe title compound was prepared

출처 및 근거

ORD 기록
ord-efba2276936e4dbeba0c17a0186321ed
출처 데이터셋
uspto-grants-2014_08
특허 번호
US08809377B2

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