Chlorosuccinimide → 6-Chloro-5-phenyl-1,2,4-triazin-3-amine

HRID 2407095노트

반응식

HRID 2407095 반응식
[C:1]1([C:7]2[N:8]=[C:9]([NH2:13])[N:10]=[N:11][CH:12]=2)[CH:6]=[CH:5][CH:4]=[CH:3][CH:2]=1.[Cl:14]N1C(=O)CCC1=O>>[Cl:14][C:12]1[N:11]=[N:10][C:9]([NH2:13])=[N:8][C:7]=1[C:1]1[CH:2]=[CH:3][CH:4]=[CH:5][CH:6]=1

참가 물질

3

반응물 2

HCID 31398ChlorosuccinimideHCID 970815-Phenyl-1,2,4-triazin-3-amine

생성물 1

HCID 866761156-Chloro-5-phenyl-1,2,4-triazin-3-amine수율 92.4%

실험 절차

6-Chloro-5-phenyl-1,2,4-triazin-3-amine (0.38 g, 65%) was prepared from 5-phenyl-1,2,4-triazin-3-amine (0.50 g, 1.99 mmol) and N-chlorosuccinimide (0.50 g, 3.7 mmol) according to the general procedure of Preparation 3.

후처리

  1. customaccording to the general procedure of Preparation 3

출처 및 근거

ORD 기록
ord-6eb20a47203c49ec9871366e2014e2a9
출처 데이터셋
uspto-grants-2014_08
특허 번호
US08809525B2

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