Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Chloro-6-(1-methylhydrazinyl)pyridazine → N'-(6-chloropyridazin-3-yl)-5-cyclohexyl-N'-methyl-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid hydrazide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Chloro-6-(1-methylhydrazinyl)pyridazine | HCID 2735815 | — |
| 반응물 | 5-Cyclohexyl-6-(2,2,2-trifluoroethoxy)nicotinic acid | HCID 71293952 | — |
| 생성물 | N'-(6-chloropyridazin-3-yl)-5-cyclohexyl-N'-methyl-6-(2,2,2-trifluoroethoxy)-3-pyridinecarboxylic acid hydrazide | HCID 71510018 | — |
반응 단계
The title compound was synthesized in analogy to Example 1 using 5-cyclohexyl-6-(2,2,2-trifluoro-ethoxy)-3-pyridinecarboxylic acid (example 12c) and 3-chloro-6-(1-methylhydrazinyl)-pyridazine (CAN 76953-33-8) as starting materials; LC-MS (UV peak area/ESI) 100.0%, 444.1408 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08648099B2 |
| 출처 데이터셋 | uspto-grants-2014_02 |
| ORD ID | ord-c7435d94371f4c3f948f87b282b5308f |
| 출처 메모 | uspto-grants-2014_02 |