Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Benzyl azide → 1-benzyl-4-(tributylstannyl)-1H-1,2,3-triazole
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Benzyl azide | HCID 12152 | — |
| 반응물 | Ethynyltributyltin | HCID 621176 | — |
| 생성물 | 1-benzyl-4-(tributylstannyl)-1H-1,2,3-triazole | HCID 68989138 | — |
반응 단계
Ethynyltributylstannane (1 mL, 3.4 mmol) and benzyl azide (0.65 mL, 5.2 mmol) were heated to 130° C. for 24 hours. The mixture was adsorbed onto silica gel, and purified by silica gel chromatography eluting with 1:4 ethyl acetate:hexanes to afford the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08648069B2 |
| 출처 데이터셋 | uspto-grants-2014_02 |
| ORD ID | ord-2cf326be26c44c51a15a50805ee623cf |
| 출처 메모 | uspto-grants-2014_02 |