tert-Octylamine → HCID 86656469, 화합물

반응식

[N:1]([CH2:4][CH2:5][C:6]1[S:7][CH:8]=[CH:9][CH:10]=1)=[C:2]=[S:3].[C:11]([NH2:19])([CH2:14][C:15]([CH3:18])([CH3:17])[CH3:16])([CH3:13])[CH3:12]>>[C:11]([NH:19][C:2]([NH:1][CH2:4][CH2:5][C:6]1[S:7][CH:8]=[CH:9][CH:10]=1)=[S:3])([CH2:14][C:15]([CH3:18])([CH3:17])[CH3:16])([CH3:13])[CH3:12]

참가 물질

반응물 2

HCID 61017tert-Octylamine

HCID 101763092-(2-Isothiocyanatoethyl)thiophene

생성물 1

HCID 86656469HCID 86656469, 화합물수율 83%

실험 절차

The procedure of step (1-1) of Example 1 was repeated except for using the compound obtained in step (2-1) (2.5 g, 15.0 mmol) and t-octyl amine (1.6 mL, 10.2 mmol), to obtain the title compound (2.5 g, 83%).

출처 및 근거

ORD 기록: ord-c833821c4062406bbd394a19d3e2b44e
출처 데이터셋: uspto-grants-2014_02
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08648111B2

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