Aminoacetaldehyde dimethyl acetal → HCID 44997787, 화합물
반응식
C([O:3][C:4](=O)[C:5]([NH:7][CH2:8][CH3:9])=[O:6])C.[CH3:11][O:12][CH:13]([O:16][CH3:17])[CH2:14][NH2:15]>CC(O)C>[CH3:11][O:12][CH:13]([O:16][CH3:17])[CH2:14][NH:15][C:4](=[O:3])[C:5]([NH:7][CH2:8][CH3:9])=[O:6]참가 물질
4
실험 절차
59.9 g (412.6 mM) of ethyl(ethylamino)(oxo)acetate and 45 ml (412.6 mM) of (2,2-dimethoxyethyl)amine, in 480 ml of 2-propanol, were stirred at room temperature for 16 h. A white precipitate was filtered, washed with 2-propanol and dried under vacuum to give 67.8 g of N-(2,2-dimethoxyethyl)-N′-ethylethanediamide.
후처리
- filtrationA white precipitate was filtered
- washwashed with 2-propanol
- customdried under vacuum
출처 및 근거
- ORD 기록
- ord-4ae09a72c3854f7fb90d09447de4dcdc
- 출처 데이터셋
- uspto-grants-2014_08
- 특허 번호
- US08815859B2
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