Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Methoxyaniline → N-(2-methoxyphenyl)-3-nitrobenzenesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Methoxyaniline | HCID 7000 | — |
| 반응물 | 3-Nitrobenzenesulfonyl chloride | HCID 8476 | — |
| 생성물 | N-(2-methoxyphenyl)-3-nitrobenzenesulfonamide | HCID 2834884 | 89.5% |
반응 단계
Using o-anisidine (1.0 ml, 8.55 mmol) and 3-nitrobenzenesulfonyl chloride (1.95 g, 8.55 mmol), the procedure of Reference Example 2 was repeated to obtain 2.36 g (89.5%) of the title compound in the form of light yellow needle crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05728835 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-df69311069264a20a142aa147b4fbb47 |
| 출처 메모 | uspto-grants-1998_03 |