Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Dimethylamine → Dimethyl(dimethylamino)ethoxysilane
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Dimethylamine | HCID 674 | — |
| 반응물 | Tetrahydrofuran | HCID 8028 | — |
| 반응물 | Bis(dimethylamino)dimethylsilane | HCID 77384 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | Dimethyl(dimethylamino)ethoxysilane | HCID 102480692 | — |
반응 단계
A 2 L 3 neck flask equipped with a magnetic stirrer, Frederich's condensor and an addition funnel was charged with 361 mls of bis(dimethylamino)dimethylsilane and an equal volume of tetrahydrofuran. At ambient temperature, 116 mls of anhydrous ethanol was added over one hour. Dimethylamine evolved. The mixture was transferred to a single neck flask and distilled. 264 g of dimethyl(dimethylamino)ethoxysilane, (b.p. 115°-118° C.), was recovered.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04491669 |
| 출처 데이터셋 | uspto-grants-1985_01 |
| ORD ID | ord-8d8c2afd79424dc693355cf7c621ac61 |
| 출처 메모 | uspto-grants-1985_01 |