4-Methoxybenzaldehyde → HCID 54069780, 화합물

반응식

[NH2:1][CH2:2][P:3](=[O:10])([O:7][CH2:8][CH3:9])[O:4][CH2:5][CH3:6].[CH3:11][O:12][C:13]1[CH:20]=[CH:19][C:16]([CH:17]=O)=[CH:15][CH:14]=1>>[CH3:11][O:12][C:13]1[CH:20]=[CH:19][C:16]([CH:17]=[N:1][CH2:2][P:3](=[O:10])([O:7][CH2:8][CH3:9])[O:4][CH2:5][CH3:6])=[CH:15][CH:14]=1

참가 물질

반응물 2

HCID 312444-Methoxybenzaldehyde

HCID 1596920Diethyl (aminomethyl)phosphonate

생성물 1

HCID 54069780HCID 54069780, 화합물수율 100%

실험 절차

Starting from 16.7 g. (0.1 mol) diethyl aminomethylphosphonate and 13.6 g. (0.1 mol) p-methoxybenzaldehyde and following the procedure described in Example 1, 28.5 g. (yield: 100%) of the desired product are obtained in the form of a yellow oil.

출처 및 근거

ORD 기록: ord-04eb668a816d407780fc670af25be8b7
출처 데이터셋: uspto-grants-1985_01
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04493931

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