Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(Trifluoromethyl)aniline → 4-methoxy-N-[2-(trifluoromethyl)phenyl]benzenesulfonamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(Trifluoromethyl)aniline | HCID 6922 | — |
| 반응물 | 4-Methoxybenzenesulfonyl chloride | HCID 7401 | — |
| 생성물 | 4-methoxy-N-[2-(trifluoromethyl)phenyl]benzenesulfonamide | HCID 755970 | 75.5% |
반응 단계
Using 2-trifluoromethylaniline (1.39 g, 8.55 mmol) and 4-methoxybenzenesulfonyl chloride (1.78 g, 8.55 mmol), the procedure of Reference Example 2 was repeated to obtain 2.14 g (75.5%) of the title compound in the form of colorless solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05728835 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-a203f03510c84376936109923b3e225b |
| 출처 메모 | uspto-grants-1998_03 |