2-Amino-2-ethyl-1,3-propanediol → 2-((6-Chrysenylmethyl)amino)-2-ethyl-1,3-propanediol hydrochloride

HRID 2413580

반응식

HRID 2413580 반응식
[ClH:1].[CH:2]1[C:19]2[CH:18]=[CH:17][C:16]3[C:7](=[CH:8][C:9]([CH2:20][NH:21][C:22]([CH3:27])([CH2:25][OH:26])[CH2:23][OH:24])=[C:10]4[C:15]=3[CH:14]=[CH:13][CH:12]=[CH:11]4)[C:6]=2[CH:5]=[CH:4][CH:3]=1.[CH:28]1C2C=CC3C(=CC(C=O)=C4C=3C=CC=C4)C=2C=CC=1.NC(CC)(CO)CO>CCO.CCOCC>[ClH:1].[CH:2]1[C:19]2[CH:18]=[CH:17][C:16]3[C:7](=[CH:8][C:9]([CH2:20][NH:21][C:22]([CH2:27][CH3:28])([CH2:23][OH:24])[CH2:25][OH:26])=[C:10]4[C:15]=3[CH:14]=[CH:13][CH:12]=[CH:11]4)[C:6]=2[CH:5]=[CH:4][CH:3]=1

참가 물질

5

반응물 3

HCID 82822-Amino-2-ethyl-1,3-propanediolHCID 124387746-ChrysenecarbaldehydeHCID 133752782-((6-Chrysenylmethyl)amino)-2-methyl-1,3-propanediol hydrochloride

생성물 1

HCID 133753422-((6-Chrysenylmethyl)amino)-2-ethyl-1,3-propanediol hydrochloride

시약·촉매·용매 1

HCID 21585056Diethyl ether ethanol용매

실험 절차

Using the reductive amination procedure described in 1B, 6-chrysenecarbaldehyde (1A) and 2-amino-2-ethyl-1,3-propanediol (Aldrich) gave 2-((6-chrysenylmethyl)amino)-2-ethyl-1,3-propanediol hydrochloride, mp 241°-243° (dec), (EtOH/Et2O), (C,H,Cl,N).

출처 및 근거

ORD 기록
ord-495790e1d65e461ca59b25dd6e355532
출처 데이터셋
uspto-grants-1988_01
특허 번호
US04719048

연결된 노트

불러오는 중…