Phosphinic acid, P-phenyl-P-(2,4,6-trimethylbenzoyl)-, sodium salt (1:1) → Phenyl(2,4,6-trimethylbenzoyl)phosphinate

HRID 2413830노트

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HRID 2413830 반응식
[CH3:1][C:2]1[CH:18]=[C:17]([CH3:19])[CH:16]=[C:15]([CH3:20])[C:3]=1[C:4]([P:6]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)(=[O:8])[O-:7])=[O:5].[Na+]>O.S(=O)(=O)(O)O>[CH3:1][C:2]1[CH:18]=[C:17]([CH3:19])[CH:16]=[C:15]([CH3:20])[C:3]=1[C:4]([P:6]([C:9]1[CH:14]=[CH:13][CH:12]=[CH:11][CH:10]=1)(=[O:7])[OH:8])=[O:5]

참가 물질

4

반응물 1

HCID 23690966Phosphinic acid, P-phenyl-P-(2,4,6-trimethylbenzoyl)-, sodium salt (1:1)

생성물 1

HCID 18674595Phenyl(2,4,6-trimethylbenzoyl)phosphinate

시약·촉매·용매 2

HCID 962Water용매HCID 1118Sulfuric Acid용매

실험 절차

46.5 parts by weight of the sodium salt of Example 1 were dissolved in 300 parts by weight of water, and 150 parts by volume of 1N sulfuric acid were added. The resulting precipitate was filtered off under suction, washed with water and dried, and 38.9 parts by weight of product were obtained.

후처리

  1. additionwere added
  2. filtrationThe resulting precipitate was filtered off under suction
  3. washwashed with water
  4. customdried
  5. custom38.9 parts by weight of product were obtained

출처 및 근거

ORD 기록
ord-2fa8484411324ff68d11f97931f1101c
출처 데이터셋
uspto-grants-1988_01
특허 번호
US04719297

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