홈MCP워크벤치Skills
홈워크벤치알림마이페이지
llms.txt · MCP 가이드개인정보처리방침 · 이용약관 · 지원v1.8.0
  1. 홈
  2. /반응

Acetyl chloride → HCID 15599411, 화합물

HRID 2414194
노트
인쇄 미리보기

반응식

HRID 2414194 반응식
[O:1]1[C:6]2[CH:7]=[CH:8][C:9]([C:11]3[CH:12]([CH3:18])[CH2:13][C:14](=[O:17])[NH:15][N:16]=3)=[CH:10][C:5]=2[NH:4][CH2:3][CH2:2]1.[C:19](Cl)(=[O:21])[CH3:20]>O1CCCC1>[C:19]([N:4]1[C:5]2[CH:10]=[C:9]([C:11]3[CH:12]([CH3:18])[CH2:13][C:14](=[O:17])[NH:15][N:16]=3)[CH:8]=[CH:7][C:6]=2[O:1][CH2:2][CH2:3]1)(=[O:21])[CH3:20]
참가 물질실험 절차후처리출처 및 근거반응 노트

참가 물질

4

반응물 2

HCID 6367Acetyl chlorideHCID 155994106-(3,4-Dihydro-1,4(2H)-benzoxazin-6-yl)-2,3,4,5-tetrahydro-5-methylpyridazin-3-one

생성물 1

HCID 15599411HCID 15599411, 화합물수율 61%

시약·촉매·용매 1

HCID 8028Tetrahydrofuran용매

실험 절차

6-(3,4-Dihydro-1,4(2H)-benzoxazin-6-yl)-2,3,4,5-tetrahydro-5-methylpyridazin-3-one was suspended in tetrahydrofuran and one equivalent of acetyl chloride was added. After one half hour at 0° C., the solvent was removed in vacuo, and the product was crystallized from ethanol in 61% yield, mp 185.5°-186° C.

후처리

  1. waitAfter one half hour at 0° C.
  2. customthe solvent was removed in vacuo
  3. customthe product was crystallized from ethanol in 61% yield, mp 185.5°-186° C.

출처 및 근거

ORD 기록
ord-edc6953ed5ea4efeaec924b9a52eac0d
출처 데이터셋
uspto-grants-1988_01
DOI
10.6084/m9.figshare.5104873.v1
특허 번호
US04721784

반응 노트

불러오는 중…

이 페이지에서참가 물질실험 절차후처리출처 및 근거반응 노트