Methanol → 1-Methoxy-2,7-octadiene

HRID 2414204

반응식

HRID 2414204 반응식
CO[CH:3]([CH2:6][CH2:7][CH2:8][CH:9]=[CH2:10])[CH:4]=[CH2:5].[CH3:11][OH:12]>[Pd](Cl)Cl>[CH3:11][O:12][CH2:10][CH:9]=[CH:8][CH2:7][CH2:6][CH2:3][CH:4]=[CH2:5]

참가 물질

4

반응물 2

HCID 887MethanolHCID 5511733-Methoxy-1,7-octadiene2회

생성물 1

HCID 5350261-Methoxy-2,7-octadiene

시약·촉매·용매 1

HCID 24290Palladium Chloride촉매

실험 절차

A process for isomerizing 3-methoxy-1,7-octadiene comprising contacting 3-methoxy-1,7-octadiene with methanol and a catalytically effective amount of a catalyst selected from the group consisting of cupric chloride and a mixture of cupric chloride and palladium chloride at a temperature in the range of between about 115° C. and 135° C. and a pressure in the range of between about 75 psig and about 125 psig whereby 8-methoxy-1,6-octadiene is formed.

출처 및 근거

ORD 기록
ord-426cf347688a4083bc6ab23c3fab2c55
출처 데이터셋
uspto-grants-1988_01
특허 번호
US04721820

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