4-Chloro-3-nitrobenzophenone → 1-{1-[2-Nitro-4-(phenylcarbonyl)phenyl]piperidin-4-yl}-1,4-dihydro-2H-3,1-benzoxazin-2-one

HRID 2414307노트

반응식

HRID 2414307 반응식
Cl.[NH:2]1[CH2:7][CH2:6][CH:5]([N:8]2[C:13]3[CH:14]=[CH:15][CH:16]=[CH:17][C:12]=3[CH2:11][O:10][C:9]2=[O:18])[CH2:4][CH2:3]1.Cl[C:20]1[CH:33]=[CH:32][C:23]([C:24]([C:26]2[CH:31]=[CH:30][CH:29]=[CH:28][CH:27]=2)=[O:25])=[CH:22][C:21]=1[N+:34]([O-:36])=[O:35]>>[N+:34]([C:21]1[CH:22]=[C:23]([C:24]([C:26]2[CH:27]=[CH:28][CH:29]=[CH:30][CH:31]=2)=[O:25])[CH:32]=[CH:33][C:20]=1[N:2]1[CH2:3][CH2:4][CH:5]([N:8]2[C:13]3[CH:14]=[CH:15][CH:16]=[CH:17][C:12]=3[CH2:11][O:10][C:9]2=[O:18])[CH2:6][CH2:7]1)([O-:36])=[O:35]

참가 물질

3

반응물 2

HCID 417434-Chloro-3-nitrobenzophenoneHCID 220630891-(4-Piperidinyl)-1,2-dihydro-4H-3,1-benzoxazin-2-one hydrochloride

생성물 1

HCID 102046651-{1-[2-Nitro-4-(phenylcarbonyl)phenyl]piperidin-4-yl}-1,4-dihydro-2H-3,1-benzoxazin-2-one

실험 절차

The title compound was prepared from 1-piperidin-4-yl-1,4-dihydro-2H-3,1-benzoxazin-2-one hydrochloride (0.3 g) and 4-chloro-3-nitrobenzophenone (0.29 g) using the method of example 1. Yield 0.25 g as a solid.

출처 및 근거

ORD 기록
ord-1565ca0f989347b49577c66d03c28130
출처 데이터셋
uspto-grants-2004_11
특허 번호
US06812226B2

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