1,1'-Carbonyldiimidazole → HCID 22644647, 화합물

HRID 2414326

반응식

HRID 2414326 반응식
[NH2:1][C:2]1[CH:7]=[CH:6][C:5]([N:8]2[CH2:13][CH2:12][CH:11]([N:14]3[C:19]4[CH:20]=[CH:21][CH:22]=[CH:23][C:18]=4[CH2:17][O:16][C:15]3=[O:24])[CH2:10][CH2:9]2)=[C:4]([Cl:25])[CH:3]=1.C(N1C=CN=C1)(N1C=CN=C1)=O.[C:38]([C:40]1([C:43](O)=[O:44])[CH2:42][CH2:41]1)#[N:39]>>[Cl:25][C:4]1[CH:3]=[C:2]([NH:1][C:43]([C:40]2([C:38]#[N:39])[CH2:42][CH2:41]2)=[O:44])[CH:7]=[CH:6][C:5]=1[N:8]1[CH2:9][CH2:10][CH:11]([N:14]2[C:19]3[CH:20]=[CH:21][CH:22]=[CH:23][C:18]=3[CH2:17][O:16][C:15]2=[O:24])[CH2:12][CH2:13]1

참가 물질

4

반응물 3

HCID 682631,1'-CarbonyldiimidazoleHCID 27332591-Cyanocyclopropanecarboxylic acidHCID 226446801-[1-(4-Amino-2-chlorophenyl)piperidin-4-yl]-1,4-dihydro-2H-3,1-benzoxazin-2-one

생성물 1

HCID 22644647HCID 22644647, 화합물

실험 절차

The title compound was prepared from the product of example 120 step (ii) (0.05 g), carbonyldiimidazole (0.025 g) and 1-cyano-1-cyclopropane carboxylic acid (0.019 g) using the method of example 115 step (i). Yield 0.003 g.

출처 및 근거

ORD 기록
ord-656ec2424c1c453d9bfa60cbcd1e00ee
출처 데이터셋
uspto-grants-2004_11
특허 번호
US06812226B2

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