Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrogen Peroxide → 4,7-Dichloroquinoline 1-oxide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrogen Peroxide | HCID 784 | — |
| 반응물 | 4,7-Dichloroquinoline | HCID 6866 | — |
| 촉매 | HCID 178477782 | HCID 178477782 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | 4,7-Dichloroquinoline 1-oxide | HCID 280096 | — |
반응 단계
A mixture of 4,7-dichloroquinoline (9.9 g, 50 mmol) and methyltrioxorhenium (80 mg, 0.32 mmol) was stirred in the mixture of hydrogenperoxide (40%, 20 mL) and dichloromethane at room temperature for 24 hours. Pale yellow solid was collected by filtration and dried under vacuum. MS (ESI(+)Q1MS m/z 215 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US06818772B2 |
| 출처 데이터셋 | uspto-grants-2004_11 |
| ORD ID | ord-e3258ff6faf74080801c127d4b5bf9d7 |
| 출처 메모 | uspto-grants-2004_11 |