Triethylamine → HCID 69669790, 화합물

HRID 241603노트

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HRID 241603 반응식
[N:1]1([CH2:6][C:7]([O:9][CH2:10]C)=[O:8])[CH:5]=[CH:4][N:3]=[N:2]1.[CH2:12](N(CC)CC)C>CO>[N:1]1([C:6](=[CH2:12])[C:7]([O:9][CH3:10])=[O:8])[CH:5]=[CH:4][N:3]=[N:2]1

참가 물질

4

반응물 2

HCID 8471TriethylamineHCID 10103365Ethyl 2-(1H-1,2,3-triazol-1-YL)acetate

생성물 1

HCID 69669790HCID 69669790, 화합물

시약·촉매·용매 1

HCID 887Methanol용매

반응 조건

온도
22 °C

실험 절차

450 g of ethyl 2-(1H-1,2,3-triazol-1-yl)acetate were dissolved in 3.5 1 of methanol, 30 g of triethylamine were added and the mixture was stirred at 22° C. for 16 h. All solvents were then distilled off under reduced pressure. This gave 410 g of the title compound as an oil.

후처리

  1. additionwere added
  2. distillationAll solvents were then distilled off under reduced pressure

출처 및 근거

ORD 기록
ord-a65d5812e32c46648999775e580451ae
출처 데이터셋
uspto-grants-2014_02
특허 번호
US08653074B2

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