4-(1H-Pyrazol-1-yl)benzaldehyde → (2E)-3-[4-(4H-1,2,4-Triazol-4-yl)phenyl]-2-propenal

반응식

[N:1]1[N:2]=[CH:3][N:4]([C:6]2[CH:13]=[CH:12][C:9]([CH:10]=O)=[CH:8][CH:7]=2)[CH:5]=1.N1(C2C=C[C:22]([CH:23]=[O:24])=CC=2)C=CC=N1>>[N:1]1[N:2]=[CH:3][N:4]([C:6]2[CH:13]=[CH:12][C:9](/[CH:10]=[CH:22]/[CH:23]=[O:24])=[CH:8][CH:7]=2)[CH:5]=1

참가 물질

반응물 2

HCID 27764774-(1H-Pyrazol-1-yl)benzaldehyde

HCID 226310064-(4H-1,2,4-Triazol-4-yl)benzaldehyde

생성물 1

HCID 22631182(2E)-3-[4-(4H-1,2,4-Triazol-4-yl)phenyl]-2-propenal

실험 절차

The title compound was prepared by a procedure analogous to Reference Example 30 by substituting 4-(4H-1,2,4-triazol-4-yl)-benzaldehyde (prepared as described in WO 98/03476) for the 4-(1H-pyrazol-1-yl)-benzaldehyde of Reference Example 30. MS 200 (M+H)+.

출처 및 근거

ORD 기록: ord-1b7772d171b648a99d652d7e8b7c6968
출처 데이터셋: uspto-grants-2004_11
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US06825170B2

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