Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethyl 1H-imidazole-1-carboxylate → HCID 178473360, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethyl 1H-imidazole-1-carboxylate | HCID 87963 | — |
| 반응물 | Methyl 3-(4-(bromomethyl)phenyl)-2-propenoate | HCID 53395294 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | HCID 178473360 | HCID 178473360 | 73.4% |
반응 단계
To 5 ml of dry acetonitrile were added 1.4 g of 1-ethoxycarbonylimidazole and 2.55 g of methyl 4-bromomethylcinnamate, the mixture was stirred for 5 hours at room temperature. The precipitated crystals were collected by filtration and recrystallized from acetonitrile/diethyl ether to yield 2.9 g of 1-ethoxycarbonyl-3-[4-(2-methoxycarbonylvinyl)benzyl]imidazolium bromide.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04469865 |
| 출처 데이터셋 | uspto-grants-1984_09 |
| ORD ID | ord-81fb1012f14e4aa5a7ad4165967cce60 |
| 출처 메모 | uspto-grants-1984_09 |