5-Bromo-1,1,1-triethoxypentane → 6-Benzyloxy-5-(5-ethoxycarbonylpentyl)-imidazo[1,5-a]pyridine

HRID 2417826노트

반응식

HRID 2417826 반응식
[CH2:1]([O:8][C:9]1[CH:10]=[CH:11][C:12]2[N:13]([CH:16]=[N:17][CH:18]=2)[C:14]=1[CH3:15])[C:2]1[CH:7]=[CH:6][CH:5]=[CH:4][CH:3]=1.Br[CH2:20][CH2:21][CH2:22][CH2:23][C:24](OCC)([O:28]CC)[O:25][CH2:26][CH3:27]>>[CH2:1]([O:8][C:9]1[CH:10]=[CH:11][C:12]2[N:13]([CH:16]=[N:17][CH:18]=2)[C:14]=1[CH2:15][CH2:20][CH2:21][CH2:22][CH2:23][C:24]([O:25][CH2:26][CH3:27])=[O:28])[C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][CH:7]=1

참가 물질

3

반응물 2

HCID 132061375-Bromo-1,1,1-triethoxypentaneHCID 133736366-Benzyloxy-5-methylimidazo[1,5-a]pyridine

생성물 1

HCID 204466596-Benzyloxy-5-(5-ethoxycarbonylpentyl)-imidazo[1,5-a]pyridine

실험 절차

The condensation of 6-benzyloxy-5-methylimidazo[1,5-a]pyridine with 5-bromo-1,1,1-triethoxypentane essentially by the procedure described in Example 1 yields 6-benzyloxy-5-(5-ethoxycarbonylpentyl)-imidazo[1,5-a]pyridine; NMR (CDCl3) 1.4 (3H), 4.17 (2H), 4.97 (2H).

출처 및 근거

ORD 기록
ord-8b66938fc2a643659ca0daf8aa3d323e
출처 데이터셋
uspto-grants-1984_09
특허 번호
US04470986

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