Acetophenone → Ethyl 2-Propyl-3-hydroxy-3-methyl-3-phenylpropionate

HRID 2418630

반응식

HRID 2418630 반응식
[C:1]([C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)(=[O:3])[CH3:2].[C:10]([O:16][CH2:17][CH3:18])(=[O:15])[CH2:11][CH2:12][CH2:13][CH3:14]>>[CH2:12]([CH:11]([C:1]([OH:3])([CH3:2])[C:4]1[CH:9]=[CH:8][CH:7]=[CH:6][CH:5]=1)[C:10]([O:16][CH2:17][CH3:18])=[O:15])[CH2:13][CH3:14]

참가 물질

3

반응물 2

HCID 7410AcetophenoneHCID 10882Ethyl valerate

생성물 1

HCID 15575787Ethyl 2-Propyl-3-hydroxy-3-methyl-3-phenylpropionate

실험 절차

A 10 milligram sample of the prepared hydroxy-ester is pyrolyzed is an open tube at 250° C. for 5 minutes. Examinationof the pyrolyzate by G.C., L.C. and T.L.C. indicates >90% decomposition to form a 1:1 mixture of acetophenone and ethyl valerate.

후처리

  1. customat 250° C.
  2. customfor 5 minutes
  3. customto form

출처 및 근거

ORD 기록
ord-1c5cd077e2a54c39b7fabe43e6d5a092
출처 데이터셋
uspto-grants-1984_09
특허 번호
US04473085

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