Water → HCID 178460683, 화합물

반응식

[Br:1][C:2]1[CH:8]=[C:7]([Br:9])[CH:6]=[C:5]([Br:10])[C:3]=1[NH2:4].Cl[C:12]([CH:14]([CH3:20])[CH2:15][P:16](Cl)(C)=[O:17])=[O:13].[OH2:21]>>[Br:1][C:2]1[CH:8]=[C:7]([Br:9])[CH:6]=[C:5]([Br:10])[C:3]=1[NH:4][C:12]([CH:14]([CH3:20])[CH2:15][PH:16](=[O:21])[OH:17])=[O:13]

참가 물질

반응물 3

HCID 962Water

HCID 89862,4,6-Tribromoaniline

HCID 54003998[2-(Chloroformyl-)2-(methyl)ethyl-]methyl phosphinic acid chloride

생성물 1

HCID 178460683HCID 178460683, 화합물

실험 절차

330 g (1 mol) of 2,4,6-tribromoaniline was reacted as described in Example 1 with 207 g (1.02 mol) of [2-(chloroformyl-)2-(methyl)ethyl-]methyl phosphinic acid chloride (prepared as described by V. K. Khairullin et al., C.A. 69, 106816 k (1968)). After hydrolysis with 6 liters of water, the resulting [2-(2,4,6-tribromophenylcarbamoyl-) 2-(methyl)ethyl-]methyl phosphinic acid was filtered off and dried at 80° C under vacuum.

후처리

filtrationthe resulting [2-(2,4,6-tribromophenylcarbamoyl-) 2-(methyl)ethyl-]methyl phosphinic acid was filtered off
customdried at 80° C under vacuum

출처 및 근거

ORD 기록: ord-fec1a8bdd3a7421f978ddd31854bd6cd
출처 데이터셋: uspto-grants-1978_08
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US04105689

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