Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,3,5-Trimethylphenol → 2,3,5-Trimethyl-phenyl ethyl ether
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,3,5-Trimethylphenol | HCID 12769 | — |
| 반응물 | 4-Ethoxy-2,3,6-trimethyl-benzyl-triphenylphosphonium chloride | HCID 86735901 | — |
| 생성물 | 2,3,5-Trimethyl-phenyl ethyl ether | HCID 20210010 | — |
반응 단계
The 4-ethoxy-2,3,6-trimethyl-benzyl-triphenylphosphonium chloride employed as the starting material is prepared by the procedure described in Example 18 by alkylation of 2,3,5-trimethylphenol to give 2,3,5-trimethyl-phenyl ethyl ether (melting point 93°-95° C), by haloformylation of the ether obtained to give 4-ethoxy-2,3,6-trimethyl-benzyl chloride (melting point 63°-64° C) and by reaction of the latter compound with triphenylphosphine.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04105681 |
| 출처 데이터셋 | uspto-grants-1978_08 |
| ORD ID | ord-895b0019d1514c44b2d71eea44267ed2 |
| 출처 메모 | uspto-grants-1978_08 |