Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Methoxybenzylamine → 4-Chloromethyl-N-(3-methoxybenzyl)benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Methoxybenzylamine | HCID 21156 | — |
| 반응물 | 4-(Chloromethyl)benzoyl chloride | HCID 70136 | — |
| 생성물 | 4-Chloromethyl-N-(3-methoxybenzyl)benzamide | HCID 19690086 | 83.9% |
반응 단계
Using 3-methoxybenzylamine (754 mg, 5.39 mmol) and 4-chloromethylbenzoyl chloride (1.17 g, 6.0 mmol), the procedure of Reference Example 13 was repeated to obtain 1.31 g (83.9%) of the title compound in the form of colorless crystals.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05728835 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-fc00450aae7f43bba3081ae919487779 |
| 출처 메모 | uspto-grants-1998_03 |