Dimethylamine → HCID 178486282, 화합물

HRID 2420371노트

반응식

HRID 2420371 반응식
CN.[CH3:3]NC.[Cl:6][C:7]1[CH:12]=[CH:11][C:10]([C:13]2[NH:14][C:15]([S:19](=[O:22])(=[O:21])[NH2:20])=[C:16](C)[N:17]=2)=[CH:9][CH:8]=1>>[Cl:6][C:7]1[CH:12]=[CH:11][C:10]([C:13]2[NH:17][CH:16]=[C:15]([S:19](=[O:22])(=[O:21])[NH:20][CH3:3])[N:14]=2)=[CH:9][CH:8]=1

참가 물질

4

반응물 3

HCID 674DimethylamineHCID 6329MethylamineHCID 178432509HCID 178432509, 화합물

생성물 1

HCID 178486282HCID 178486282, 화합물수율 4.4%

실험 절차

Substituting aqueous methylamine for the dimethylamine in Example 3 2-(4-chlorophenyl)-4-methyl-sulfamoylimidazole, melting at 246°-248°, was obtained (4.4% yield).

후처리

  1. customwas obtained (4.4% yield)

출처 및 근거

ORD 기록
ord-a22b0e0f4b594b0bb0947737771bffce
출처 데이터셋
uspto-grants-1978_08
특허 번호
US04110456

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