Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
O-Cresol → Methyl 3-(4-((3-(2-methylphenoxy)benzyl)oxy)phenyl)propanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | O-Cresol | HCID 335 | — |
| 반응물 | 3-Bromobenzaldehyde | HCID 76583 | — |
| 반응물 | Benzenepropanoic acid, 4-hydroxy-, methyl ester | HCID 79706 | — |
| 반응물 | [3-(2-Methylphenoxy)phenyl]methanol | HCID 23082899 | — |
| 생성물 | Methyl 3-(4-((3-(2-methylphenoxy)benzyl)oxy)phenyl)propanoate | HCID 23083053 | — |
반응 단계
The title compound was synthesized in the same manner as in Example 277 from methyl 3-(4-hydroxyphenyl)propanoate and [3-(2-methylphenoxy)phenyl]methanol (synthesized in the same manner as in Reference Example 201 from o-cresol and 3-bromobenzaldehyde (mixture with side product)) (preparative HPLC (gradient cycle A) was used for purification). colorless oil (yield 28%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07960369B2 |
| 출처 데이터셋 | uspto-grants-2011_06 |
| ORD ID | ord-3476422b94804a7e9a1fd304ed91910e |
| 출처 메모 | uspto-grants-2011_06 |