Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → 2-Chloro-2-oxoethyl 4'-chlorobiphenyl-4-sulfonate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 2-(4'-Chlorobiphenyl-4-ylsulfonyloxy)acetic acid | HCID 86628700 | — |
| 생성물 | 2-Chloro-2-oxoethyl 4'-chlorobiphenyl-4-sulfonate | HCID 86628702 | — |
반응 단계
A mixture of acid 13 (100 mg, 0.306 mmol) and thionyl chloride (1 ml) was heated at reflux for 1.5 h. The excess thionyl chloride was removed in vacuo and the resulting pale yellow/white solid dried under high vacuum at 50° C. for 1.5 h. The product acid chloride 14 was used without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07960434B2 |
| 출처 데이터셋 | uspto-grants-2011_06 |
| ORD ID | ord-d8e1d267abee4aeba70658dc436a7c38 |
| 출처 메모 | uspto-grants-2011_06 |