Hydroxylamine → HCID 136346368, 화합물
반응식
[Br:1][C:2]1[C:11]2[N:10]=[CH:9][CH:8]=[CH:7][C:6]=2[C:5]([CH:12]=O)=[CH:4][CH:3]=1.[NH2:14][OH:15]>C(O)C>[Br:1][C:2]1[C:11]2[N:10]=[CH:9][CH:8]=[CH:7][C:6]=2[C:5]([CH:12]=[N:14][OH:15])=[CH:4][CH:3]=1참가 물질
4
실험 절차
To a stirred solution of 8-bromo-5-quinolinecarboxaldehyde (i.e. the product from Step B) (1.7 g, 7.1 mmol) in ethanol (30 mL) was added an aqueous solution of hydroxylamine (0.7 mL, 50% in water). After stirring at room temperature for 2 h, the reaction mixture was concentrated under reduced pressure to provide the title compound as a pale yellow solid (1.8 g).
후처리
- concentrationthe reaction mixture was concentrated under reduced pressure
출처 및 근거
- ORD 기록
- ord-8ec5a5b5f8dc4ae0a775174bf8af00fc
- 출처 데이터셋
- uspto-grants-2011_06
- 특허 번호
- US07964204B2
반응 노트
불러오는 중…