Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Toluene → HCID 18179455, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Toluene | HCID 1140 | — |
| 반응물 | Dimethylformamide | HCID 6228 | — |
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | 4'-Fluorobiphenyl sulfonic acid | HCID 18179513 | — |
| 생성물 | HCID 18179455 | HCID 18179455 | — |
반응 단계
4′-Fluorobiphenyl sulfonic acid (3 g) was refluxed in thionyl chloride (30 mL) with a catalytic quantity of DMF (0.5 mL) for 4 hours. Toluene was added and the solvents evaporated under vacuum to give the title compound as an amorphous solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07964643B2 |
| 출처 데이터셋 | uspto-grants-2011_06 |
| ORD ID | ord-9c4a67b14b954527a80f0abf8b367bc8 |
| 출처 메모 | uspto-grants-2011_06 |