Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Nitrobenzoic Acid → N-[3-(methylsulfanyl)phenyl]-4-nitrobenzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Nitrobenzoic Acid | HCID 6108 | — |
| 반응물 | Benzenamine, 3-(methylthio)- | HCID 15693 | — |
| 생성물 | N-[3-(methylsulfanyl)phenyl]-4-nitrobenzamide | HCID 873432 | 85.3% |
반응 단계
Using 3-methylthioaniline (1.40 ml, 11.0 mmol) and 4-nitrobenzoic acid (1.67 g, 10.0 mmol), the procedure of Reference Example 16 was repeated to obtain 2.46 g (85.2%) of the title compound in the form of yellow powder.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05728835 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-bac4f35022814f6eaa0f9cad74b4ef8c |
| 출처 메모 | uspto-grants-1998_03 |